This book is part of an acclaimed continuing series designed to provide authoritative reviews on recent developments and applications of well-established techniques in the field of electroanalytical chemistry. The 26th volume explores three topics: nanoscale scanning electrochemical microscopy, electrochemical applications of scanning ion conductance microscopy, and electrode surface modification using diazonium salts. Each volume provides the necessary background and a starting point for graduate students undertaking related research projects as well as practicing analytical chemists concerned with electroanalytical techniques and their fundamental principles.